Recipe for:
Heroin purification to nearly USP
by Steve J. Quest [squest@moonwatcher.avrtech.com]
from alt.drugs, Wed May 18, 1994
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[Erowid Note: We received an unconfirmed note saying that if this procedure
were used on fentanyl or other synthetic "heroin substitutes", the resulting
chemical would be dangerous to use. We are looking for verifying details.]
This is as complete and as accurate as I can remember, it has been something
like 10 years since I have used heroin. The process I used for purification
was straight forward. Diacetylmorphine can exist in two forms, an insoluable
base, or a soluable salt. Often it contained a plethera of other agents like
pieces of broken glass, pieces of foil, dirt, wood, metal, mannitol, lactose,
maltose, sand, you get the idea. The first stage of the process I used was
to make sure the diacetylmorphine I received was totally converted to a soluable
hydrochloride salt. The heroin I usually received was a brown powdered heroin,
sometimes off white, very little vinegar smell. Today all you can find is
a black crud that reeks with a vinegar (acetic) odor. The way I made sure
it was a soluable salt was to drop enough 28% hydrochloric acid to make it
wet. This insured that I would not waste any of the available drug, but would
remove most if not all of the cut. I think that it would be better for me
to detail it in a procedural manner. FYI, hydrochloric acid can be purchased
in gallon jugs at hardware stores under the name Muriatic acid, 28%.
First weigh out one gram of heroin from the stock you received from your
supplier. Place this gram into a 13 x 100mm test tube. Add a few drops of
28% hydrochloric acid until it is evenly damp. Allow to react for a minute
or two. Next add 5 ml distilled water, place your thumb over the end and carefully
shake to dissolve all that will dissolve into the water. Allow the insoluables
to settle. Using a pipette, remove and transfer as much of the liquid to
a fresh test tube leaving the solids behind. Dispose of the undissolved remains
in the first test tube. Slowly add via pipette, one drop at at time, ammonium
hydroxide (water clear household ammonia) until the white precipitate ceases
production. Add several more drops at this point just to be sure. Shake gently
to be sure that all the solution is evenly ammoniated. The solution should
look milky. Now add 100 ml ethyl ether (some kinds of diesel starting fluids,
read the label) to a 150 ml beaker. Dump the milky liquid into the ether
and stir briskly and allow the water to settle and collect on the bottom.
The water will turn clear. Using a glass pipette, remove this water from
the bottom of the beaker and dispose of.
Now mix up a solution of 5ml 28% hydrochloric acid and 5ml distilled water
and add this to the ether in the beaker. Stir briskly keeping as much acid/water
suspended as possible for several minutes. Allow the water/acid to collect
on the bottom of the beaker. Using a glass pipette, remove this water layer
from the bottom of the ether and transfer to a glass petri dish. Transfer
the ether back to its storage bottle for reuse. It will still contain small
amounts of heroin base, so don't throw it out. Recycle! Slowly add small portions
of sodium bicarbonate (baking soda) to the water/acid solution in the petri
until you don't notice any more bubbles being formed. Place the glass on
a warm surface, and allow to evaporate. The residue will be diacetylmorphine
hydrochloride and salt. Table salt is a by-product of the reaction and will
not hurt you at all when injected. Scrape up the residue and weigh it. Yield
from one gram of smack (yea, we called it that) would be anything from 100
to 300 mg, rarely more. Place 100 mg of this powder in a test tube, add 10
cc sterile isotonic water for injection (available OTC at drug stores) and
heat to boiling. Transfer this liquid while still hot using a syringe (available
OTC at some drug stores) to a 10 ml rubber stoppered empty sterile ampoule
(available OTC at drug stores).
To use this drug which is 10mg/ml, extract with a sterile syringe as much
drug as you wish to use. 10 mg would send me flying believe it or not. 2.5mg
(1/4 cc) was usually enough to keep me "happy" and was my normal dose. 20mg
was the most I could take safely in my opinion, and was a waste of drug and
money. Normally, for most 150-170 lb males, 2.5 mg is more than enough in
my opinion. Using heroin in this manner avoids the problems associated with
"street use" and will keep your body healthy and safe, reducing the risk of
disease and overdosage.
My memory is pretty good, and I think I covered all the bases here, but
I may have made a mistake somewhere. Overall I think this is an accurate
method, to the best of my ability to remember.
Originally archived by the Hyperreal Drug Archives. Hosted by Erowid as
of Oct, 1999.
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Last Modified - Tue, Apr 19, 2005 Used by Erowid without permission of author
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